КФУ. Карточка публикации. Sensitive voltammetric quantification of carminic acid in candies using selenium dioxide nanoparticles based electrode

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SENSITIVE VOLTAMMETRIC QUANTIFICATION OF CARMINIC ACID IN CANDIES USING SELENIUM DIOXIDE NANOPARTICLES BASED ELECTRODE

Форма представления

Статьи в зарубежных журналах и сборниках

Год публикации

2022

Язык

английский

Авторы, сотрудники КФУ

Зиятдинова Гузель Камилевна, автор

Авторы, студенты КФУ

Кавиева Лия Радиковна, автор

Библиографическое описание на языке оригинала

Kavieva, L. Sensitive voltammetric quantification of carminic acid in candies using selenium dioxide nanoparticles based electrode / L. Kavieva, G. Ziyatdinova // Food Chem. – 2022. – V. 386. – Article 132851. – 8 p.

Аннотация

Carminic acid is a food colorant which concentration has to be controlled due to the possible negative health effects. Sensitive voltammetric method is developed for carminic acid determination using electrode modified with SeO2 nanoparticles (SeO2 NPs) and hexadecyltriphenylphosphonium bromide (HDTPPB) acting as dispersive agent for nanoparticles and electrode surface co-modifier. SeO2 NPs of 37–45 nm are uniformly distributed at the electrode increasing its electroactive area (41 ? 2 vs. 8.9 ? 0.2 mm2 for bare glassy carbon electrode (GCE)). Electrochemical impedance spectroscopy data confirm an 18.3-fold decrease of charge transfer resistance compared to GCE (12.7 ? 0.3 vs. 232 ? 7 kΩ, respectively). In differential pulse mode, the linear dynamic ranges of carminic acid are 0.010–2.5 and 2.5–10 μmol L−1 with a detection limit of 3.4 nmol L−1. The method is successfully employed in candies and lozenges for sore throat treatment. The approach is simple, reliable, and can be used as an alternative to chromatography in routine analysis.

Ключевые слова

Food colorants, carminic acid, voltammetric detection, modified electrodes, nanoparticles, surfactants

Название журнала

FOOD CHEMISTRY

URL

https://www.scopus.com/inward/record.uri?eid=2-s2.0-85127182352&doi=10.1016%2fj.foodchem.2022.132851&partnerID=40&md5=52b4841685c66af34920d120bd86d831

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https://repository.kpfu.ru/?p_id=266209

Полная запись метаданных

Поле DC	Значение	Язык
dc.contributor.author	Зиятдинова Гузель Камилевна	ru_RU
dc.contributor.author	Кавиева Лия Радиковна	ru_RU
dc.date.accessioned	2022-01-01T00:00:00Z	ru_RU
dc.date.available	2022-01-01T00:00:00Z	ru_RU
dc.date.issued	2022	ru_RU
dc.identifier.citation	Kavieva, L. Sensitive voltammetric quantification of carminic acid in candies using selenium dioxide nanoparticles based electrode / L. Kavieva, G. Ziyatdinova // Food Chem. – 2022. – V. 386. – Article 132851. – 8 p.	ru_RU
dc.identifier.uri	https://repository.kpfu.ru/?p_id=266209	ru_RU
dc.description.abstract	FOOD CHEMISTRY	ru_RU
dc.description.abstract	Carminic acid is a food colorant which concentration has to be controlled due to the possible negative health effects. Sensitive voltammetric method is developed for carminic acid determination using electrode modified with SeO2 nanoparticles (SeO2 NPs) and hexadecyltriphenylphosphonium bromide (HDTPPB) acting as dispersive agent for nanoparticles and electrode surface co-modifier. SeO2 NPs of 37–45 nm are uniformly distributed at the electrode increasing its electroactive area (41 ? 2 vs. 8.9 ? 0.2 mm2 for bare glassy carbon electrode (GCE)). Electrochemical impedance spectroscopy data confirm an 18.3-fold decrease of charge transfer resistance compared to GCE (12.7 ? 0.3 vs. 232 ? 7 kΩ, respectively). In differential pulse mode, the linear dynamic ranges of carminic acid are 0.010–2.5 and 2.5–10 μmol L−1 with a detection limit of 3.4 nmol L−1. The method is successfully employed in candies and lozenges for sore throat treatment. The approach is simple, reliable, and can be used as an alternative to chromatography in routine analysis.	ru_RU
dc.language.iso	ru	ru_RU
dc.subject	Food colorants	ru_RU
dc.subject	carminic acid	ru_RU
dc.subject	voltammetric detection	ru_RU
dc.subject	modified electrodes	ru_RU
dc.subject	nanoparticles	ru_RU
dc.subject	surfactants	ru_RU
dc.title	Sensitive voltammetric quantification of carminic acid in candies using selenium dioxide nanoparticles based electrode	ru_RU
dc.type	Статьи в зарубежных журналах и сборниках	ru_RU